Parr-instrument 6200 Uživatelský manuál

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Operating Instruction Manual
No. 442M
9
6200
Oxygen Bomb Calorimete
r
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Strany 1 - Oxygen Bomb Calorimete

Operating Instruction Manual No. 442M9 6200Oxygen Bomb Calorimeter

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116200Calorimeter Operating Instruction ManualOverview The 6200 Calorimeter has been designed to provide the user with: • A traditional design ca

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12 6200Calorimeter Operating Instruction ManualFull Micro-processor Based Process Control Full Micro-processor Based Data Acquisition and Handling

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136200Calorimeter Operating Instruction ManualFilling the Jacket ReservoirPowerConnectionJacket Cooling Water Connection The 6200 Calorimeter is co

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14 6200Calorimeter Operating Instruction ManualJacket Cooling Water Connection Continued Oxygen Filling Connection Printer and Balance Connections 2

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156200Calorimeter Operating Instruction ManualRetightening Swagelok Tube Fittings When Swagelok Tube Fittings are used, the instructions for ins

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16 6200Calorimeter Operating Instruction Manual Figure 2-1 6200 Calorimeter Back Panel 2-42

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176200Calorimeter Operating Instruction Manual2 Line 1 & 2 – Maximum length of 10 feet -¼” OD, Polyurethane (Part Number HJ0025TB035) Line 3

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18 6200Calorimeter Operating Instruction Manual Open Loop Configurations Figure 2-4 Figure 2-5 2-6 2

Strany 10 - 6200Calorimeter O

196200Calorimeter Operating Instruction ManualStandardizing the Calorimeter The calorimeter must be accurately standardized prior to actually perfo

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20 6200Calorimeter Operating Instruction Manual2This page intentionally left blank. 2-8

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36200Calorimeter Operating Instruction ManualPreface I Scope...

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216200Calorimeter Operating Instruction ManualControl Keys All calorimeter configurations and operations are handled by a menu-driven system operat

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22 6200Calorimeter Operating Instruction Manual3 This page intentionally left blank.3-2

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236200Calorimeter Operating Instruction Manual The program in the 6200 Calorimeter can be extensively modified to tailor the unit to a wide variety

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24 6200Calorimeter Operating Instruction ManualRevising Default Settings The default parameters of the 6200 Calorimeter can be changed to guarante

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256200Calorimeter Operating Instruction ManualFigure 4- 1 6200 Factory Default Settings Calorimeter Operation Operating Mode Determination Bomb

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26 6200Calorimeter Operating Instruction Manual4 Data Entry Controls Prompt for Bomb ID ON Weight Entry Mode Touch Screen Acid Entry Mode Touch

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276200Calorimeter Operating Instruction ManualOperating the Filling Connection Detailed Instructions for preparing the sample and charging the 1108

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28 6200Calorimeter Operating Instruction ManualOperating the Calorimeter All operations required to standardize the 6200 Calorimeter, or test an un

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296200Calorimeter Operating Instruction Manual4. Set the bucket in the calorimeter. Attach the lifting handle (421A) to the two holes in the side

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30 6200Calorimeter Operating Instruction Manual10. Remove all unburned pieces of fuse wire from the bomb electrodes; straighten them and measure the

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4 6200Calorimeter Operating Instruction Manual Operating Instructions 5-1 Operating the 1108 Oxygen Bomb...

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316200Calorimeter Operating Instruction Manual Particle Size and Moisture Content. Solid samples burn best in an oxygen bomb when reduced to 60 m

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32 6200Calorimeter Operating Instruction ManualCombustion CapsulesCoarse Samples Non-volatile samples to be tested in Parr oxygen bombs are weighed

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336200Calorimeter Operating Instruction ManualCorrosive Samples 5 The 1108 Oxygen Bomb is made of a corrosion resistant alloy designed to withstan

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34 6200Calorimeter Operating Instruction Manual Use the following procedure when filling and handling any of these tape-sealed sample holders: •

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356200Calorimeter Operating Instruction Manual Final reports for each test can be obtained whenever the operator is prepared to enter any required

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36 6200Calorimeter Operating Instruction Manual This page intentionally left blank.6 6-2

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376200Calorimeter Operating Instruction ManualReportOption SelectionReport Generation The 6200 Calorimeter can transmit its stored test data in eit

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38 6200Calorimeter Operating Instruction Manual The displayed files can be sorted by sample ID number, by type, by status or by date of test by sim

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396200Calorimeter Operating Instruction ManualClearing Memory The 6200 Calorimeter will hold data for 1000 tests in its memory. These tests may be

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40 6200Calorimeter Operating Instruction Manual This page intentionally left blank.88-2

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56200Calorimeter Operating Instruction ManualAppendix B – Calculations B-1 Calculating the Heat of Combustion...

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416200Calorimeter Operating Instruction Manual Under normal usage the 1108 Parr Oxygen Bomb will give long service if handled with reasonable care.

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42 6200Calorimeter Operating Instruction ManualThe replacement of protective fuses for the 6200 Calorimeter should be performed by qualified personn

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436200Calorimeter Operating Instruction Manual A / D Initialization Failed. Shortly after power is applied to the calorimeter controller and the op

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44 6200Calorimeter Operating Instruction Manual This page intentionally left blank.99-4

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456200Calorimeter Operating Instruction Manual The settings and controls are organized into nine main sections or pages which comprise the Main Men

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46 6200Calorimeter Operating Instruction Manual Setup. Press this key to access the Temperature Plot Setup Menu, which has many keys tha

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476200Calorimeter Operating Instruction Manual Time Units. Toggles between minutes and seconds. Bucket Plot Color. Toggles between: • Red • Green •

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48 6200Calorimeter Operating Instruction ManualOperating Controls Menu Method of Operation. Offers an operating mode of either dynamic

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496200Calorimeter Operating Instruction ManualProgram Information and Control Menu Calibrate Touchscreen. This key prompts the user to touch the sc

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50 6200Calorimeter Operating Instruction ManualProgram Information and Control MenuContinuedCalibration Data and Controls Menu Save User Default Set

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6 6200Calorimeter Operating Instruction Manual Figures 2-1 6200 Calorimeter Back Panel ...

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516200Calorimeter Operating Instruction ManualCalibration and Data Controls Menu Continued EE Max Std Deviation. Displays the maximum relative stan

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52 6200Calorimeter Operating Instruction ManualThermo-chemical Corrections MenuPrint Standardization Runs. Will print all of the tests that have bee

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536200Calorimeter Operating Instruction ManualCalculation Factors. Accesses sub-menu, Calculation Factors which sets a number of options for the way

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54 6200Calorimeter Operating Instruction ManualData Entry Controls Menu Prompt for Bomb ID. In the ON position the controller will pro

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556200Calorimeter Operating Instruction ManualAuto Preweigh ID Controls. Accesses sub-menu, used to automatically assign Sample ID numbers when a se

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56 6200Calorimeter Operating Instruction Manual Communication Controls. Accesses sub-menus which set the communications protocols for t

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576200Calorimeter Operating Instruction ManualBalance Port (RS232). Accesses sub-menu, Balance Port Communications. Balance Type. This key toggl

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58 6200Calorimeter Operating Instruction ManualFile Management MenuAPPENDIX A Run Data File Manager - This key activates the File Manager. The File

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596200Calorimeter Operating Instruction ManualDiagnostics Menu APPENDIX A Allows the user to test many of the components and subsystems of the c

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60 6200Calorimeter Operating Instruction Manual This page intentionally left blank.APPENDIX A8-2

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76200Calorimeter Operating Instruction ManualScope This manual contains instructions for installing and operating the Parr 6200 Calorimeter. For ea

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616200Calorimeter Operating Instruction ManualCalculating the Heat of CombustionGeneral Calculations The 6200 Calorimeter will automatically make a

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62 6200Calorimeter Operating Instruction ManualThermochemical Corrections Nitric Acid Correction. In the high pressure oxygen environment within

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636200Calorimeter Operating Instruction Manual Current ASTM, ISO, and British Standard Methods differ on their treatment of the nitric and sulfuric

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64 6200Calorimeter Operating Instruction Manual• Total acid is the amount of base required to titrate the bomb washings (milliliters). • Nitric ac

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656200Calorimeter Operating Instruction ManualAcid and Sulfur CorrectionsContinued Users may find it convenient to enter a fixed value for the acid

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66 6200Calorimeter Operating Instruction Manual In the ASTM treatment, the correction for acid formation assumes that all the acid titrated is nitr

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676200Calorimeter Operating Instruction Manualm Spiking SamplesConversion to Other Moisture BasesConversion to Net Heat of Combustion It is someti

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68 6200Calorimeter Operating Instruction Manual This page intentionally left blank.APPENDIX BB-8

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696200Calorimeter Operating Instruction ManualStandard Materials The Energy Equivalent Factor. The term “standardization”, as used here, denotes

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70 6200Calorimeter Operating Instruction Manual The 6200 Calorimeter includes a provision for calculating and using a mean energy equivalent for ea

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8 6200Calorimeter Operating Instruction ManualPREFACE Explanation of Symbols I On position O Off position ~ Alternating Current (AC) This CAUTION

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716200Calorimeter Operating Instruction ManualPrinter Port Balance Port RS232C Connections The 6200 Calorimeter is also equipped with an RS232C port

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72 6200Calorimeter Operating Instruction ManualSartoriousBalanceInterface Field Length polarity 1 space 1 data 8 space 1 stability 2 CR 1 LF 1 T

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736200Calorimeter Operating Instruction ManualField Length data 9 CR 1 The data field should consist of 9 numeric characters (0 through 9, +, - a

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74 6200Calorimeter Operating Instruction Manual Table D-2 6200 Calorimeter Run Data Template Field Desc

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756200Calorimeter Operating Instruction Manual Calorimeter test data can be transferred to an Ethernet network connected computer using the FTP File

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76 6200Calorimeter Operating Instruction Manual The following screenshot illustrates the contents of the calorimeter data directory as presented by

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776200Calorimeter Operating Instruction Manual The calorimeter offers a web server service. Test reports can be viewed with a web browser using a UR

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78 6200Calorimeter Operating Instruction Manual Clicking on the Sample Data tab displays a list of reports currently in the instrument memory.

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796200Calorimeter Operating Instruction Manual Clicking on any given report will provide a display as follows.

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80 6200Calorimeter Operating Instruction ManualBar Code PortNetwork Data Devices The use of barcodes in the laboratory has become a highly accurat

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96200Calorimeter Operating Instruction ManualSafety Information To avoid electrical shock, always: 1. Use a properly grounded electrical outlet of

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816200Calorimeter Operating Instruction Manual Should you need assistance in the operation or service of your instrument, please contact the Techni

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82 6200Calorimeter Operating Instruction Manual This page intentionally left blank.APPENDIX EE-2

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836200Calorimeter Operating Instruction Manual APPENDIX F 6200 CALORIMETER PARTS LIST Principal Asse

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84 6200Calorimeter Operating Instruction ManualParts List for Temperature Control Assembly Item Description 1281DD 1417E 538VB 252HWHJ 280HWHJ A12

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856200Calorimeter Operating Instruction ManualParts List for 6200 Stirrer Motor and Drive Item Description 1285DD 1241DD2 1242DD A1268DD Mount, Mot

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86 6200Calorimeter Operating Instruction Manual Figure F-1 6200 Oxygen Bomb Calorimeter Cutaway Front F-4A

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876200Calorimeter Operating Instruction Manual Figure F-2 6200 Oxygen Bomb Calorimeter Cutaway Rear F-5 A

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88 6200Calorimeter Operating Instruction Manual F-6Figure F-3 A1279DD Control Schematic APPENDIX F

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896200Calorimeter Operating Instruction Manual F-7 Figure F-4 Oxygen Solenoid Assembly & Fittings A

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90 6200Calorimeter Operating Instruction Manual F-8Figure F-5 Water Tank Assembly APPENDIX F

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10 6200Calorimeter Operating Instruction Manual These steps are offered to help the user become familiar with, install, operate and develop the full

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916200Calorimeter Operating Instruction Manual F-9 Figure F-6 A1311DD Circulating Pump Assembly with Fittings APPENDIX F

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92 6200Calorimeter Operating Instruction ManualF-10Figure F-7 Temperature Control Assembly with Fittings APPENDIX F

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936200Calorimeter Operating Instruction ManualAPPENDIX F Figure F-8 A1284DD2 Stirrer Hub Assembly F-11

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94 6200Calorimeter Operating Instruction Manual APPENDIX FF-12 Figure F-9 Stirrer Motor Assembly F-12

Strany 94 - Revision 01/29/10

Revision 01/29/10 PARR INSTRUMENT COMPANY 211 Fifty - Third Street Moline, Illinois 61265 USA 309 / 762-7716 800 / 872-7720 Fax 309 / 7

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