Parr-instrument 6200 Uživatelský manuál stáhnout pdf (Strana 4)

6200Calorimeter O

eratin

Instruction Manual

Appendix B – Calculations B-1

Calculating the Heat of Combustion............................................................ B-1

General Calculations................................................................................... B-1

Thermochemical Corrections ...................................................................... B-2

ASTM and ISO Methods Differ.................................................................... B-3

Acid and Sulfur Corrections ........................................................................ B-4

ASTM Treatment for Acid and Sulfur .......................................................... B-6

ISO Calculations ......................................................................................... B-6

Spiking Samples ......................................................................................... B-7

Conversion to Other Moisture Bases .......................................................... B-7

Conversion to Net Heat of Combustion....................................................... B-7

Appendix C- Standardization C-1

Standardizing the Calorimeter..................................................................... C-1

Standard Materials...................................................................................... C-1

Automatic Statistical Calculations ............................................................... C-2

Appendix D - Communication Interfaces D-1

Printer Port.................................................................................................. D-1

Balance Port................................................................................................ D-1

Mettler 011/012 Balance Interface .............................................................. D-1

Sartorius Balance Interface......................................................................... D-2

Generic Interface......................................................................................... D-3

Run Date Template..................................................................................... D-4

Ethernet Interface........................................................................................ D-5

Bar Code Port ............................................................................................. D-10

Network Data Devices................................................................................. D-10

Appendix E - Technical Service E-1

Return for Repair......................................................................................... E-1

Appendix F – 6200 Calorimeter Parts & Diagrams F-1

Principal Assemblies in Calorimeter............................................................ F-1

Parts List for A1279DD Controller Assembly .............................................. F-1

Parts List for Temperature Control Assembly ............................................. F-2

Parts List for A1284DD2 Stirrer Hub Assembly .......................................... F-2

Spare and Installation Parts List ................................................................. F-2

Parts List for Water Tank Assembly............................................................ F-3

Parts List for Cooling Water Supply ............................................................ F-3

Parts List for Oxygen Filling System ........................................................... F-3

Parts List for 6200 Stirrer Motor and Drive.................................................. F-3

F-1 6200 Oxygen Bomb Calorimeter Cutaway Front ............................. F-4

F-2 6200 Oxygen Bomb Calorimeter Cutaway Rear.............................. F-5

F-3 A1279DD Control Schematic........................................................... F-6

F-4 Oxygen Solenoid Assembly............................................................. F-7

F-5 Water Tank Assembly...................................................................... F-8

F-6 A1311DD Circulating Pump Assembly ............................................ F-9

F-7 Temperature Control Assembly .......................................................F-10

F-8 A1284DD2 Stirrer Hub Assembly ....................................................F-11

F-9 Stirrer Motor Assembly ....................................................................F-12

TABLE OF CONTENTS

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