Parr-instrument Series 4590 Uživatelský manuál

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399M
4590
Micro Bench Top Reactors
Operating Instruction Manual
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Strany 1 - Operating Instruction Manual

399M4590 Micro Bench Top ReactorsOperating Instruction Manual

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4590 Micro ReactorsParr Instrument Company10IDENTIFY THE VALVESGas Inlet ValveThe gas inlet valve is easily identified when the vessel is open by notin

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4590 Micro Reactorswww.parrinst.com11OTHER VESSEL HEAD FITTINGSSafety Rupture DiscThere is a safety rupture disc attached to the head that is intended

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4590 Micro ReactorsParr Instrument Company12Air MotorVariable stirring speeds from 100 to 2000 rpm with no spark hazard can be obtained by replacing t

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Noteswww.parrinst.com13

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4590 Micro ReactorsParr Instrument Company14HOW TO USE THE VESSELRemovable VesselsAlways remove removable vessels from the support stand before attem

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4590 Micro Reactorswww.parrinst.com15Gas ConnectionsFor a gas connection to the vessel, use the A495HC pressure hose (A506HC in high pressure reactors

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4590 Micro ReactorsParr Instrument Company16MAINTENANCEGeneral Maintenance Notes1. Periodically inspect all electrical wiring and pres-sure connectio

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4590 Micro Reactorswww.parrinst.com17Periodic Pressure TestsEach cylinder used in a Parr stirred reactor is tested under hydrostatic pressure to the

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4590 Micro ReactorsParr Instrument Company18SERIES 4590 VESSEL PARTS LISTSStandard Vessel Fittings (3000 psig / 350 °C)Standard Reaction Vessel Parts

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4590 Micro Reactorswww.parrinst.com19Heads*Part No. Description Code2432HC Head RV FG2902HC Head RV OR2772HC Head FH FG2774HC Head FH OR1432HC Head SC

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4590 Micro ReactorsParr Instrument Company20R/D ASSEMBLYW/526HC_STYLE RD302VBADFEMALECONNA138CAMALE CONNA2067HC_STYLETHERMOWELLA1357E_STYLET/CA451VBVA

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4590 Micro Reactorswww.parrinst.com21High Pressure Reaction Vessel Parts ListConsult the itemized list for your reactor provided along with this manua

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4590 Micro ReactorsParr Instrument Company22THERM429HC2KLGASKET, GRAFOIL40HCADAPTER, A SKT X1/4 NPTFVALVE, STRAIGHTPLUG, HEAD 1/4 NPTM1443HC2NIPPLE, H

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4590 Micro Reactorswww.parrinst.com233340HC2HEADHigh Pressure / High Temperature Reaction Vessel Parts ListConsult the itemized list for your reactor

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4590 Micro ReactorsParr Instrument Company24Vessel Heaters (Standard Stand Configuration)Part No. DescriptionA3240HC9EB Heater Assembly, TW, 700W, 115V

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4590 Micro Reactorswww.parrinst.com25Support Stands4591/4592 Micro Reactor with 1/8 hp Variable Speed Motor1.49 (DOWN POSITION)2.05 (UP POSITION)SW51F

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4590 Micro ReactorsParr Instrument Company264591/4592 Micro Reactor with Variable Speed 1/4 HP and Explosion Proof Motors(SEE MOTOR TABLE)56C MOUNT MO

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4590 Micro Reactorswww.parrinst.com274593 Micro Reactor with Fixed Head

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399M R06 01/22/15

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4590 Micro Reactorswww.parrinst.com3PREFACE 4Scope 4Related Instructions 4Intended Usage 4Safety Information 4General Specifications 4Elect

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4590 Micro ReactorsParr Instrument Company4PREFACEScopeThese instructions describe the installation, opera-tion and maintenance of Parr Series 4590 Be

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4590 Micro Reactorswww.parrinst.com5Explanation of SymbolsII On position, full power heater switchI On position, half power heater switchO Off Positio

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Parr Instrument Company64590 Micro ReactorsUser’s ResponsibilityAll Parr Reactors and pressure vessels are designed and manufactured with great care t

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4590 Micro Reactorswww.parrinst.com7Parr Series 4590 Micro Reactors are furnished with two structural options in addition to the size, pressure range,

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Parr Instrument Company84590 Micro ReactorsINSTALLATIONPressure and Temperature LimitsThe working pressure and temperature at which any reactor or pre

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4590 Micro Reactorswww.parrinst.com9Assemble The ReactorThese reactors require at least 10 sq. ft. of workspace in a well-ventilated area with conven

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