
6400 Calorimeter Instruction Manual
TABLE OF CONTENTS
TABLE OF CONTENTS ................................................................................................1-1
PREFACE......................................................................................................................1-1
Scope.........................................................................................................................1-1
Purpose......................................................................................................................1-2
Explanation of Symbols..............................................................................................1-2
Safety Information......................................................................................................1-3
INSTALLATION.............................................................................................................2-1
Consumables, Utilities and Power Requirements......................................................2-2
Electrical Connection .................................................................................................2-2
Water Connection ......................................................................................................2-3
Gas Connection .........................................................................................................2-4
Bomb Exhaust Connections.......................................................................................2-5
Communication Connections .....................................................................................2-5
Printer Connections....................................................................................................2-7
Balance Connections .................................................................................................2-7
Mettler 011/012 Interface .....................................................................................2-8
Sartorious Interface .............................................................................................2-8
Generic Interface..................................................................................................2-8
Bar Code Port ............................................................................................................2-8
Computer Connections ..............................................................................................2-9
QUICK START...............................................................................................................3-1
OPERATION..................................................................................................................4-1
Menu System .............................................................................................................4-1
Menu Keys .................................................................................................................4-1
Control Keys...............................................................................................................4-2
Programming..............................................................................................................4-2
Default Settings..........................................................................................................4-2
Sample Preparation ...................................................................................................4-3
Sample Size...........................................................................................................4-3
Particle Size and Moisture Content........................................................................4-3
Sample Types ........................................................................................................4-4
Combustion Aids....................................................................................................4-6
Combustion Capsules............................................................................................4-6
Test Process ..............................................................................................................4-7
Loading the sample................................................................................................4-7
Closing the bomb ...................................................................................................4-7
Fill Cycle.................................................................................................................4-8
Pre-Period ..............................................................................................................4-9
Bomb Firing..........................................................................................................4-10
Post-Period ..........................................................................................................4-10
Cool / Rinse..........................................................................................................4-11
Drain.....................................................................................................................4-12
MENU DESCRIPTIONS.................................................................................................5-1
Main Menu .................................................................................................................5-1
Calorimeter Operation Menu......................................................................................5-1
Temperature vs. Time Plot.........................................................................................5-2
Temperature Plot Setup Menu...................................................................................5-2
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