Parr-instrument 6300 Uživatelský manuál stáhnout pdf (Strana 4)

Parr Instrument Company

TABLE OF CONTENTS

4

APPENDIX B

C

ALCULATIONS — 71

Calculating the Heat of Combustion — 71

General Calculations — 71

Thermochemical Corrections — 71

Fuse Correction — 73

Acid and Sulfur Corrections — 73

ASTM Treatment for Acid and Sulfur — 74

ISO Calculations — 75

Spiking Samples — 75

Conversion to Net Heat of Combustion — 75

APPENDIX C

S

TANDARDIZATION — 77

Standardizing the Calorimeter — 77

Standard Materials — 77

Automatic Statistical Calculations — 77

APPENDIX D

C

OMMUNICATIONS INTERFACES — 81

USB Port — 81

Balance and Port Input Driver Specifications — 81

Mettler 011/012 Balance Interface — 81

Sartorius Balance Interface — 81

Generic Interface — 82

Ethernet Interface — 83

Samba Server Feature (Optional) — 84

Bar Code Port — 92

Network Data Services — 92

APPENDIX E

T

ECHNICAL SERVICE — 93

Return for Repair — 93

APPENDIX F

P

ARTS LISTS & DRAWINGS — 95

Principal Assemblies in Calorimeter — 95

A1250DD2 Controller Assembly — 96

A1251DD Oxygen Solenoid Assembly — 96

A1252DD Water Solenoid Assembly — 96

A1257DD Water Regulator Assembly — 97

A1258DD Temperature Control Assembly — 97

A1260DD Water Level Assembly — 97

A1264DD Air Can Assembly — 98

A1267DD Accessory/Installation Kit — 99

A1265DD Bucket and Stirrer Tube Assembly — 99

6300 Stirrer Motor and Drive — 100

A1255DD Bucket Stirrer Assembly — 100

A1266DD Cover Assembly — 100

6309B Spare Parts Kit — 101

1136 and 1136CL Oxygen Bomb — 103

1138 and 1138CL Oxygen Bomb — 105

FIGURES

Figure 2-1

Swagelok Tube Fittings — 15

Figure 2-2

6300 Calorimeter Back Panel — 16

Figure 2-3

Closed Loop Configuration with 6520A — 17

Figure 2-4

Closed Loop Configuration with 1564 — 17

Figure 2-5

Open Loop Configuration with 1552 — 18

Figure 2-6

Open Loop Configuration — 18

Figure 4-1

6300 Factory Default Settings — 24

Figure 5-1

Fill Flow Diagram — 28

Figure 5-2

Cotton Thread Assembly — 29

Figure 5-3

Pre-period/Post-period — 30

Figure 5-4

Rinse & Cool Flow Diagram — 32

Figure 5-5

Drain Flow Diagram — 34

Figure 5-6

Combustion Capsule with Adhesive Tape Seal — 37

Figure F-1

Parts Diagram for the 1136 and 1136CL Oxygen

Bombs — 102

TABLES

Table B-1

Settings for ISO & BSI Methods — 74

Table C-1

Calorimeter Control Limit Values in J/g When

Benzoic Acid is Used as a Test Sample — 78

Table C-2

Calorimeter Control Limit Values in cal/g When

Benzoic Acid is Used as a Test Sample — 79

Table C-3

Calorimeter Control Limit Values in BTU/lb When

Benzoic Acid is Used as a Test Sample — 80

Table D-1

6300 Data File Naming Convention — 82

Table D-2

6300 Calorimeter Run Data Template — 82

APPENDIX G

B

OMB RINSE CONTAINER ASSEMBLY — 127

Overview — 127

Concept of Operation — 127

Connection — 127

Operation — 127

1 2 3 4 5 6 7 8 9 ... 129 130

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